Z-9-DODECEN-1-YL ACETATE
- CasNo:16974-11-1
Product Description
Top Quality Chinese Manufacturer supply 16974-11-1 Z-9-DODECEN-1-YL ACETATE
- Molecular Formula: C14H26 O2
- Molecular Weight: 226.359
- Vapor Pressure: 0.00114mmHg at 25°C
- Refractive Index: 1.4439 (22℃)
- Boiling Point: 300.1°Cat760mmHg
- Flash Point: 96.5°C
- PSA： 26.30000
- Density: 0.881g/cm3
- LogP: 4.24640
Z-9-DODECEN-1-YL ACETATE(Cas 16974-11-1) Usage
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Synthesis Reference(s) |
Tetrahedron Letters, 21, p. 1433, 1980 DOI: 10.1016/S0040-4039(00)92738-2 |
InChI:InChI=1/C14H26O2/c1-3-4-5-6-7-8-9-10-11-12-13-16-14(2)15/h4-5H,3,6-13H2,1-2H3/b5-4-
16974-11-1 Relevant articles
Simple stereospecific synthesis of the insect sex pheromones of Cossus cossus, Eupoecilia ambiguella and Orgyia pseudotsugata
Cahiez,Alexakis,Normant
, p. 1433 - 1436 (1980)
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SYNTHESIS OF PHEROMONE DERIVATIVES VIA Z-SELECTIVE OLEFIN METATHESIS
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, (2021/12/28)
Disclosed herein are methods for synthes...
Method for synthesizing grassland spodoptera litura sex pheromone active ingredients
-
, (2020/07/02)
The invention belongs to the technical f...
PRODUCTION OF FATTY OLEFIN DERIVATIVES VIA OLEFIN METATHESIS
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Paragraph 0386; 0404, (2017/06/12)
In one aspect, the invention provides a ...
SYNTHESIS OF Z-OLEFIN-CONTAINING LEPIDOPTERAN INSECT PHEROMONES
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Paragraph 0185; 0186, (2013/09/12)
The present invention is directed to met...
16974-11-1 Process route
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91856-11-0
Δ9 -dodecen-1-ol
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108-24-7
acetic anhydride
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35148-19-7
(E)-9-dodecenyl acetate
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16974-11-1
(Z)-9-dodecenyl acetate
| Conditions | Yield |
|---|---|
|
With
pyridine;
Yield given. Yields of byproduct given. Title compound not separated from byproducts;
|
|
|
With
pyridine;
In
dichloromethane;
at 20 ℃;
for 17h;
Overall yield = 87 %; Overall yield = 0.18 g;
|
48 % de
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925-90-6
ethylmagnesium bromide
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-
108-24-7
acetic anhydride
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98752-55-7
(Z)-2-(8-phenylthiodec-9-enyloxy)tetrahydro-2H-pyran
-
-
35148-19-7
(E)-9-dodecenyl acetate
-
-
16974-11-1
(Z)-9-dodecenyl acetate
| Conditions | Yield |
|---|---|
|
1,2-bis(diphenylphosphino)ethane nickel(II) chloride;
Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
1.) ether, 12 h, room temp., 2.) 80 deg C, 15 h;
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16974-11-1 Upstream products
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29541-97-7
9-acetoxynonal
-
6228-47-3
n-propyltriphenylphosphonium bromide
-
91856-11-0
Δ9 -dodecen-1-ol
-
108-24-7
acetic anhydride
16974-11-1 Downstream products
-
29541-97-7
9-acetoxynonal
-
56219-03-5
(Z)-9-Dodecenal